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The secondary-electron yield depends not only on the ion species and the beam energy but is also sensitive to surface impurities. Long irradiations lead to a reduction of the secondary-electron yield in a region around the beam position. Therefore, calibration of the SEETRAM yield has to be repeated for every experiment.
The calibration of the SEETRAM current with respect to the primary beam intensity can most easily be performed by counting the particles with an additional detector system. At FRS there are two detectors available to determine the calibration factor of the SEETRAM: a Scintillator (SCI) and a Ionisation Chamber (IC).

 

Calibration with a scintillator

In this case a scintillation detector is inserted into the beam in the target area in addition to the SEETRAM. The scintillation detector is much thicker than the SEETRAM detector and is therefore only inserted during the calibration procedure.
The Figure 1 show the counting rate measured by the scintillator (SCI) and the SEETRAM as a function of time for a Pb beam at 500 AMeV. The spill structure of the beam is to be recognize in both part of the figure. In the analysis of the data the number of particles measured by the SCI are integrated over one spill as well as the number of SEETRAM counts inside the same spill.
seesci_spills.gif (10952 bytes) Figure 1. Counting rate measured by the scintillator SCI01 (upper part) and SEETRAM (lower part) as a function of time for a lead beam at 500 AMeV.
Plotting the number of particles inside the spills against the corresponding SEETRAM counts and making a linear fit, Figure 2, the SEETRAM calibration factor is obtained. Nevertheless, the response of the SCI depends strongly on the beam intensity and for  fast particle counting up to counting rates of 106 per second saturation effects in the SCI start to be remarkable.

 

scisat.gif (5291 bytes) Figure 2. Number of particles inside the spills measured with SCI01 as a function of the corresponding SEETRAM counts (open dots). Blue line represents the linear fit to data that gives the SEETRAM calibration factor.
 

As a consequence, the overlap region where it is possible to count the particles with the scintillator and to determine the SEETRAM current is rather small. The sensitivity limit of the SEETRAM (about 10-12 As = 6.25 106 e) corresponds to 3 104 uranium projectiles or 7.8 105 argon projectiles. Another drawback of using the SCI for the SEETRAM calibration is that its light output suffers from radiation damages, and must be renewed from time to time.

Calibration with an ionisation chamber (IC)
To replace the scintillation detector, an IC has been used as an alternative detector for the SEETRAM calibration . It does not show any radiation damages. The anode of the ionisation chamber is connected to a preamplifier by a capacity and to a current digitiser by a resistance. The signals of the preamplifier are fed into an amplifier and counted with the help of a discriminator and a scaler. In this way the IC is applied simultaneously for counting single particles, and for measuring the ionisation current induced in the counting gas.

 

Figure 3. SEETRAM calibration with an ionisation chamber (IC). IC can be used for measuring the ionisation current induced by the passage of a beam and for counting single particles.
 

The SEETRAM calibration is performed in two steps. First, the current in the ionisation chamber is calibrated by a particle counting. Secondly, the SEETRAM current is calibrated with respect to the ionisation current. The Figure 4 shows the particle counting rate measured by the IC (upper part) and the current due to the passage of Pb ions through the IC (lower part) as a function of time.

iccurrpart_spills.gif (11208 bytes) Figure 4. As a function of time are shown the particle counting rate (upper part) and the current induced by the passage of 500 AMeV lead ions (lower part) through the IC.
 

By integrating over the spills and making a linear fit on the two quantities, the first calibration factor is obtained. By doing the same operations with the spills corresponding to the current in the IC and the current in the SEETRAM (see Figure 5) the second calibration factor is determined. A suitable combination of the two factors gives the SEETRAM calibration constant.

SEEIC_SPILLS.gif (11722 bytes) Figure 5. Current counting rate in the IC (upper part) and the counting rate in the SEETRAM (lower part) as a function of time. 
 

The first step of the calibration is limited by counting losses due to pile up but particle counting up to 105 per second is possible. Therefore the first calibration must be performed at low beam intensities.

 

CALIC.gif (4484 bytes) Figure 6. Open dots - induced current in the IC vs. number of particles in a given spill (also measured by the IC). Blue line - linear fit to the measured data resulting in a calibration factor current IC / particles IC.
 

The second calibration is influenced by recombination losses of the ionisation current. Recombination is proportional to the product of the density of ions and the density of electrons inside the chamber. Since each of them is proportional to the beam intensity recombination effects can be considered in the analysis by fitting a second-order polynomial to the ionisation current as a function of the SEETRAM current. The calibration factor is given by the linear coefficient of the fit. As we can see in the Figure 7, the parabolic fit works only in the lowest range of intensity.

 

CALSEE.gif (4511 bytes) Figure 7. Open dots - current induced in the IC vs. number f counts in the SEETRAM. Blue line - parabolic fit to these data.
 

The two steps of the calibration for Pb ions at 500 AMeV can be seen in the Figure 8:

 

PARABLEFIT.gif (4774 bytes)

PARABOLFIT.gif (5750 bytes)

Figure 8. Two steps SEETRAM calibration with a ionisation chamber.
 

The quotient of the slope of the linear fit of the first figure and the first order coefficient of the parabolic fit give a SEETRAM calibration constant of 237 Pb ions/SEETRAM count. For the same projectile, the ionisation current is about 1000 times higher than the SEETRAM current. Therefore, the overlap regions for the two calibrations are quite large.

Noise

There are two sources of noise: statistical noise and periodic electric fields of accelerator components. Current measurement and particle counting are influenced by noise in different ways. Since there is no galvanic connection, the integrated currents from SEETRAM and ionisation chamber are not disturbed by any noise. However, the function of the current digitiser may be disturbed if the first stages saturate. Since all noise signals are bipolar, it is important to tune the offset of the current digitizers high enough to ensure that the digital outputs of the current digitisers never stop. If this happens, any information on the magnitude of the current during this time is lost! In particular, strong bipolar noise signals have been observed at the beginning and at the end of the extraction cycle. 
In particle counting, any noise signal may erroneously be interpreted as a particle. Therefore the noise signals, both statistical and periodic, must be considerably smaller than the particle signals. In order to avoid periodic noise, ground loops should be avoided and the detectors should be properly shielded. 
In the analysis of the data the positive offset of the Current Digitiser must be accurately subtracted before integrating over the spills.

 

Operation limits of both calibration methods

As it has been shown before, the detectors involved in the calibration depend strongly on the beam intensity. All detectors must be operated in an intensity range in which its behaviour is well known in order to avoid  important systematic errors.
The SCI works well up to counting rates around 105 particles per second where saturation effects start to be remarkable. The particle counting of the IC is as well limited due to pile up in the preamplifier.
On the other hand, the current produced in both the SEETRAM and the IC must be higher than 10-12 Ampere in order to distinguish the signals from the positive offset of the Current Digitizer.
Finally, recombination effects in the IC cannot be described by a parabolic fit for high intensities.
The limits of operation we recommend for the two calibration methods are displayed in the next table:

DETECTOR PROPERTY

LOWER LIMIT

EFFECT

UPPER LIMIT

EFFECT

 SCI particle counting           NO!           105/s   Saturation < 1%
 IC particle counting           NO!           104/s   Pile up < 1%
 IC current          10-12A Offset uncertainty <1%         10-7A  Recombination losses     < 10%
 SEETRAM current          10-12A Offset uncertainty <1%         NO!!

 

The last considerations are graphically represented for different ions in the Figure 9.

 

Seecal.gif (15351 bytes) Figure 9. Operational limits of the SCI (left) and the IC (right) calibration methods. Different lines represent the regions of applicability of different methods: black line - SEETRAM current, blue line - particles counting by SCI, green line - particles counting by IC, red line - current measured by IC.
 

The calibration constants for Zr, Ca and Ne were taken from Brohm's model. In all cases a SEETRAM sensitivity of 10-10 is assumed.
The figures in the left side correspond to the SCI calibration method. The blue line represents the region of applicability of the SCI and the black one the region of applicability of the SEETRAM in terms of counting rates. For heavy ions like Pb, the operation ranges of both detectors overlap. However, for lower charges the overlapping region decreases, since the intensity needed to produce a secondary electron current that overcomes the sensitivity limit ( 10-12 Ampere) increases. The limit case occurs for Zr, for lighter ions like Ca and Ne there is no overlapping and this method is not longer applicable with the desired accuracy.
In the right column are the figures related to the IC method. The green and the red line represent the range of applicability of the particle counting and the current digitizer of the IC respectively. The range of applicability of the SEETRAM is like before represented in black. The ionisation current has a large dynamic range which widely overlaps with the sensitivity range of the SEETRAM. However, depending on the size of the ionization chamber and the counting gas,  particle counting is not possible for very light ions below  Z=10 since the pulses of the single ions cannot be resolved from the background in the preamplifier. Nevertheless in this case one still could do the calibration by combining the two detectors SCI and IC, using the SCI for the particle counting.

 

Trigger conditions for the calibration
During the intensity calibration of the SEETRAM, all relevant signals are registered by scalers. In order to write the status of the scalers in periodic intervals on tape, the data acquisition is triggered by a clock, 1 Hertz or 10 Hertz. A 1 Hertz clock should also be used as an additional trigger, also during the normal measurements, in order to regularly read the scalers, also during beam pauses.

 

Measurement of the extraction efficiency of SIS for Pb-beam at different energies

In April '99 the SEETRAM was calibrated for Pb ions at 250, 500 and 1000 AMeV and the extraction efficiency of SIS was measured.
At 500 MeV the calibration was done with both calibration methods. The SCI method gave a value of 231 Pb ions/SEETRAM count for the calibration constant and the IC method 237 Pb ions/SEETRAM count. Both results are inside the error limits if we assume an statistic error of 2%, which is the accuracy needed for precise cross section measurements.
Once the SEETRAM is calibrated we can determine beam intensity. By comparing it with the current measured inside SIS we obtain the extraction efficiency. The procedure is shown for Pb ions at 500 AMeV in the Figure 10.

 

SE01_SECS.gif (7411 bytes) Figure 10. Different accelerator spills measured by the SEETRAM for different intensities as a function of time.
 

Figure 10 shows different accelerator spills measured by the SEETRAM for different intensities as a function of time. The first horizontal line gives the number of the SEETRAM counts inside the spills, the second horizontal line gives the number of Pb ions measured in SIS for the same spills. The Figure 11 represents these quantities (the SEETRAM counts are transformed into the absolute intensity). The slope of the linear fit gives an extraction efficiency of approximately 73%. 

 

EFFICIENCY.gif (4958 bytes) Figure 11. Number of particles measured at the target area of FRS vs. number of particles measured in SIS (open dots). Linear fit to these data (blue line) gives the extraction efficiency.
 

The following table sumarizes the results of these measurements. In all cases the SEETRAM sensitivity was set to 10-10:

   ENERGY

                               CALIBRATION METHOD

CALIBRATION FACTOR                                EXTRACTION    EFFICIENCY            COMMENTS
  250 AMeV                SCI 162 Pb ions/SEETRAM count              65%               Spill length~1s
  250 AMeV                SCI 168 Pb ions/SEETRAM count             67%               Spill length~5s
  250 AMeV                SCI 168 Pb ions/SEETRAM count             76%         New extraction setup
  500 AMeV                SCI 231 Pb ions/SEETRAM count             73%  
  500 AMeV                 IC 237 Pb ions/SEETRAM count             75%  
1000 AMeV                SCI 307 Pb ions/SEETRAM count             72%  

 

In general the extraction efficiency of SIS rounds 70%.

For these data we assume an statistical error of 2%. The possibility of additional systematic errors must be considered as well. Figure 12 represents in detail the lowest intensity range of the current in the IC as a function of the number of particles in the IC. These data were measured for two different sensitivities 10-9and 10-10. To plot them together the values of the ionisation current taken at 10-9sensitivity were multiplied by factor 10. The figure shows that there is a clear discontinuity in the transition from one sensitivity to the next which might be due to a wrong sensitivity adjustment of the current digitizer.

 

CALMUSIC.gif (3632 bytes) Figure 12. Effect of a wrong sensitivity adjustment.
Comparison with theoretical predictions

Based on experimental data measured at 1000 MeV Brohm et al. developed a model which predicts the secondary electron yield for all energies and ion species.
In the figure 13, the number of secondary electrons produced in the SEETRAM by Pb ions at different energies that follow from our calibration (black dots, left scale) are represented along with the theoretical predictions made by Brohm (white dots, left scale). Experimental and theoretical data agree very well for high energies but differ as decreasing the energy of the projectiles. In addition the energy loss of the ions in the SEETRAM is represented (triangles, right scale). The effects of the velocity of the ion seem not to be well reproduced by Brohm's model.

 

GRAFIK.gif (5261 bytes) Figure 13. Number of secondary electrons produced in the SEETRAM by a passage of lead ions as a function of the beam energy. Full dots and open dots (left scale) represent measured and calculated data, respectively. Open triangles (right scale) show the energy loss of the ions in the SEETRAM.
 

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